HuagongsheHuagongshe Chemistry Print Report · For research reference only
Phosphorus oxychloride → 4,8-Dichloro-2,3-dimethylquinoline
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Phosphorus oxychloride | HCID 24813 | — |
| Reactant | HCID 178432245 | HCID 178432245 | — |
| Product | 4,8-Dichloro-2,3-dimethylquinoline | HCID 59631546 | — |
Reaction Steps
Prepared according to procedure S using 8-chloro-2,3-dimethylquinolin-4-ol (1.14 g, 5.49 mmol) in POCl3 (7 mL). The resulting precipitate was collected by filtration to have 4,8-dichloro-2,3-dimethylquinoline. Mass Spectrum (ESI) m/e=227 (M+1).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08765940B2 |
| Source dataset | uspto-grants-2014_07 |
| ORD ID | ord-f112101a30b648baac5f89a0e5a09489 |
| Source note | uspto-grants-2014_07 |