HuagongsheHuagongshe Chemistry Print Report · For research reference only
Sodium Carbonate → HCID 67285251, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Sodium Carbonate | HCID 10340 | — |
| Reactant | Phenylboronic Acid | HCID 66827 | — |
| Reactant | 2,4-Dichloro-3-methyl-1,8-naphthyridine | HCID 22082661 | — |
| Catalyst | HCID 178418397 | HCID 178418397 | — |
| Product | HCID 67285251 | HCID 67285251 | — |
Reaction Steps
Prepared according to procedure F using 2,4-dichloro-3-methyl-1,8-naphthyridine (150 mg, 0.704 mmol), phenylboronic acid (86 mg, 0.704 mmol), sodium carbonate (149 mg, 1.408 mmol) and Pd(PPh3)4. Product used without further purification in the next step. Mass Spectrum (ESI) m/e=255.0 (M+1).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08765940B2 |
| Source dataset | uspto-grants-2014_07 |
| ORD ID | ord-664cd460c72544a79f4932dc698a8595 |
| Source note | uspto-grants-2014_07 |