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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1618892Generated: October 30, 2026

Hydrochloric Acid → HCID 86673626, compound

https://huagongshe.com/reaction/1618892

Reaction equation

Participants

RoleNameHCIDCharge
ReactantHydrochloric AcidHCID 313—
ReactantHydroxyamine hydrochlorideHCID 443297—
ReactantHCID 68285598HCID 68285598—
SolventPyridineHCID 1049—
ProductHCID 86673626HCID 86673626111.1%

Reaction Steps

0.46 g of 1-[2-(quinolin-3-yloxy)-phenyl]-ethanone and 0.15 g of hydroxylamine hydrochloride were dissolved in 3 ml of pyridine and then the mixture was stirred for 24 hours at room temperature. After the reaction mixture was treated with dilute hydrochloric acid and separated with ethyl acetate, the organic layer was concentrated to obtain 0.54 g of 1-[2-(quinolin-3-yloxy)-phenyl]-ethanone oxime (Compound Number 23).

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS08772200B2
Source datasetuspto-grants-2014_07
ORD IDord-03a2ef0a39264b7aa968e6684263b5bb
Source noteuspto-grants-2014_07