HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrochloric Acid → HCID 86673626, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrochloric Acid | HCID 313 | — |
| Reactant | Hydroxyamine hydrochloride | HCID 443297 | — |
| Reactant | HCID 68285598 | HCID 68285598 | — |
| Solvent | Pyridine | HCID 1049 | — |
| Product | HCID 86673626 | HCID 86673626 | 111.1% |
Reaction Steps
0.46 g of 1-[2-(quinolin-3-yloxy)-phenyl]-ethanone and 0.15 g of hydroxylamine hydrochloride were dissolved in 3 ml of pyridine and then the mixture was stirred for 24 hours at room temperature. After the reaction mixture was treated with dilute hydrochloric acid and separated with ethyl acetate, the organic layer was concentrated to obtain 0.54 g of 1-[2-(quinolin-3-yloxy)-phenyl]-ethanone oxime (Compound Number 23).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08772200B2 |
| Source dataset | uspto-grants-2014_07 |
| ORD ID | ord-03a2ef0a39264b7aa968e6684263b5bb |
| Source note | uspto-grants-2014_07 |