HuagongsheHuagongshe Chemistry Print Report · For research reference only
m-Chloroperbenzoic acid → HCID 70968088, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | m-Chloroperbenzoic acid | HCID 70297 | — |
| Reactant | HCID 86673627 | HCID 86673627 | — |
| Solvent | Chloroform | HCID 6212 | — |
| Product | HCID 70968088 | HCID 70968088 | 100% |
Reaction Steps
0.2 g of 3-(1,1-dimethylindan-7-yloxy) quinolone was dissolved in 5 mL of chloroform, and 0.2 g of m-CPBA (70%) was added and stirred overnight at room temperature. After the reaction mixture was diluted with chloroform and washed with saturated sodium bicarbonate water, magnesium sulfate was added to dry the resultant. The solvent was evaporated under reduced pressure to obtain 0.2 g of 3-(1,1-dimethylindan-7-yloxy) quinoline-N-oxide.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08772200B2 |
| Source dataset | uspto-grants-2014_07 |
| ORD ID | ord-0b943fd774d34f6d8313822c3fdef6c3 |
| Source note | uspto-grants-2014_07 |