HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1619136Generated: October 30, 2026
1,1-Dimethoxyethyl(dimethyl)amine → HCID 178464895, compound
https://huagongshe.com/reaction/1619136
Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | 1,1-Dimethoxyethyl(dimethyl)amine | HCID 87835 | — |
| Reactant | HCID 58170464 | HCID 58170464 | — |
| Product | HCID 178464895 | HCID 178464895 | 100% |
Reaction Steps
A mixture of 3-fluoro-5-iodo-4-methylbenzamide (preparation 50b) and (1,1-dimethoxyethyl)dimethylamine was heated at 120° C. in a sealed tube. After 2 hours, the reaction mixture was cooled and the solvent was evaporated under reduced pressure to give the title compound (1.84 g, 100%) as an oil.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| Patent number | US08772288B2 |
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| Source dataset | uspto-grants-2014_07 |
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| ORD ID | ord-35180b23496b4f0a89d5e1d6527c36fe |
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| Source note | uspto-grants-2014_07 |
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