Methanol → HCID 58574125, compound

Participants

Reaction Steps

A solution of 6-bromo-9-oxo-1,2,3,9-tetrahydropyrrolo[2,1-b]quinazolin-1-yl benzenesulfonate (300 mg, 0.69 mmol) and potassium carbonate (290 mg, 2.1 mmol) in methanol (80 mL) was stirred at reflux for 2 h. After it was cooled to room temperature, the mixture was concentrated and purified by silica-gel chromatography to give the desired product. MS (ESI): 309, 311 (MH+).

Provenance & Evidence