HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 53399353, compound → HCID 68296580, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 53399353 | HCID 53399353 | — |
| Reactant | HCID 178418361 | HCID 178418361 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Methanol | HCID 887 | — |
| Solvent | Tetrahydrofuran | HCID 8028 | — |
| Product | HCID 68296580 | HCID 68296580 | — |
Reaction Steps
A mixture of 472 mg 7-methoxy-5-nitro-1H-indole-2-carboxylic acid and 0.1 g Pd/C 10% in 10 ml methanol and 20 ml tetrahydrofuran was stirred for 2 h at ambient temperature under a pressure of 3 bar of hydrogen. The catalyst was filtered and the filtrate was evaporated to obtain brown solid.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08772305B2 |
| Source dataset | uspto-grants-2014_07 |
| ORD ID | ord-2df76852a88b4016b4c1ff9aed1d7e1f |
| Source note | uspto-grants-2014_07 |