HuagongsheHuagongshe Chemistry Print Report · For research reference only
Phosphorus oxychloride → HCID 86675897, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Phosphorus oxychloride | HCID 24813 | — |
| Reactant | HCID 178517733 | HCID 178517733 | — |
| Product | HCID 86675897 | HCID 86675897 | — |
Reaction Steps
A mixture of 10 g I.28 (4-(4-chloro-pyridin-2-yl)-pyrimidin-2-ol) in 100 ml phosphorus oxychloride was stirred for 3 h at reflux. The solvent was evaporated and the crude 8.1 was used in the next step without purification.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08772305B2 |
| Source dataset | uspto-grants-2014_07 |
| ORD ID | ord-14de2c354341478a982e74fc897a7228 |
| Source note | uspto-grants-2014_07 |