HuagongsheHuagongshe Chemistry Print Report · For research reference only
Water → HCID 11300149, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Water | HCID 962 | — |
| Reactant | Sodium Hydroxide | HCID 14798 | — |
| Reactant | HCID 486623 | HCID 486623 | — |
| Reactant | HCID 16092376 | HCID 16092376 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 11300149 | HCID 11300149 | 100.6% |
Reaction Steps
Compound 32 (3.0 g, 10 mmol), 100 ml of water, 50 ml of ethanol, and NaOH (2.0 g, 50 mmol) were added into a 100 ml round-bottom flask. The mixture was refluxed for 2 h. The subsequent operational steps were conducted according to those for synthesizing compound 3 to obtain light yellow solids (2.7 g, 99%), and mp 182-184° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08772311B2 |
| Source dataset | uspto-grants-2014_07 |
| ORD ID | ord-bc261a7630944d658475bb6d7c60af98 |
| Source note | uspto-grants-2014_07 |