Benzoyl Peroxide → HCID 67466145, compound

Participants

Reaction Steps

3.00 g (10.41 mmol) 6-bromo-2-p-tolyl-benzoxazole are stirred together with 1.90 g (10.68 mmol) N-bromosuccinimide, 10.00 mg (0.04 mmol) dibenzoylperoxide and 60 ml carbon tetrachloride for 2 h at 90°. The reaction mixture is filtered through kieselguhr, then the solv. is eliminated by rotary evaporation in vacuo and the residue is recrystallised from petroleum ether.

Provenance & Evidence