HuagongsheHuagongshe Chemistry Print Report · For research reference only
Piperidine → HCID 67464358, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Piperidine | HCID 8082 | — |
| Reactant | HCID 67466145 | HCID 67466145 | — |
| Solvent | Tetrahydrofuran | HCID 8028 | — |
| Product | HCID 67464358 | HCID 67464358 | — |
Reaction Steps
200 mg (545 μmol) 6-bromo-2-(4-bromomethyl-phenyl)-benzoxazole and 100 mg (1174 μmol) piperidine are stirred for 20 min in 4 ml THF at RT, the solv. is eliminated by rotary evaporation in vacuo. The residue is dissolved in ether and extracted with water, the org. phase is dried on magnesium sulphate and the solv. is eliminated completely in vacuo.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08772323B2 |
| Source dataset | uspto-grants-2014_07 |
| ORD ID | ord-b43d6901751741d89b846ebe1dbe158e |
| Source note | uspto-grants-2014_07 |