HuagongsheHuagongshe Chemistry Print Report · For research reference only
Acetyl chloride → (R)-3-methoxy-dihydro-furan-2,5-dione
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Acetyl chloride | HCID 6367 | — |
| Reactant | (R)-methoxy-succinic acid | HCID 5325475 | — |
| Product | (R)-3-methoxy-dihydro-furan-2,5-dione | HCID 86689062 | — |
Reaction Steps
260 mg (1.76 mmol) (R)-methoxy-succinic acid are stirred together with 5 ml acetyl chloride for 2 days at RT, then the acetyl chloride is eliminated by rotary evaporation in vacuo.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08772323B2 |
| Source dataset | uspto-grants-2014_07 |
| ORD ID | ord-19823be922e347f4a76b1f5ab5467e58 |
| Source note | uspto-grants-2014_07 |