HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrochloric Acid → HCID 67466209, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrochloric Acid | HCID 313 | — |
| Reactant | Water | HCID 962 | — |
| Reactant | Lithium Hydroxide | HCID 3939 | — |
| Reactant | HCID 67465972 | HCID 67465972 | — |
| Solvent | 1,4-Dioxane | HCID 31275 | — |
| Product | HCID 67466209 | HCID 67466209 | — |
Reaction Steps
100 mg (285 μmol) methyl 4-methyl-3-(2-phenyl-benzoxazole-6-carbonyl)-pentanoate, 10 mg (418 μmol) lithium hydroxide, 1 ml of water and 1 ml dioxane are stirred for 24 h at RT. The reaction mixture is acidified with conc. hydrochloric acid and extracted with diethyl ether, the org. phase is dried on magnesium sulphate and the solv. is eliminated by rotary evaporation i.V.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08772323B2 |
| Source dataset | uspto-grants-2014_07 |
| ORD ID | ord-d0498a0cfb034f8e8d2ea3cd979c56ac |
| Source note | uspto-grants-2014_07 |