HRID1619949

反应详情

EQUATION

反应方程式

HRID 1619949 的结构方程式

AUXILIARIES

试剂、催化剂与溶剂

2

PROCEDURE

实验过程

235 mg (552 μmol) 6-[2-(4-benzyloxy-phenyl)-benzoxazol-6-yl]-5-ethyl-4,5-dihydro-2H-pyridazin-3-one are hydrogenated together with 50 mg palladium on charcoal 10% and 50 ml of methanol at RT and 3.45 bar hydrogen pressure for 2.5 h, then the catalyst is filtered off and the filtrate is evaporated down completely i.V.

WORKUP

后处理

  1. filtrationthe catalyst is filtered off
  2. customthe filtrate is evaporated down completely i.V