HuagongsheHuagongshe Chemistry Print Report · For research reference only
(2-Thiophen-2-yl-benzoxazol-6-yl)methanol → 2-Thiophen-2-yl-benzoxazole-6-carbaldehyde
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | (2-Thiophen-2-yl-benzoxazol-6-yl)methanol | HCID 67466243 | — |
| Catalyst | HCID 178418406 | HCID 178418406 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | 2-Thiophen-2-yl-benzoxazole-6-carbaldehyde | HCID 82036610 | — |
Reaction Steps
3.7 g (16.0 mmol) (2-thiophen-2-yl-benzoxazol-6-yl)-methanol are dissolved in 200 ml DCM, 15.0 g (10.78 mmol) manganese dioxide are added and the suspension is stirred overnight at RT. The next day the suspension is filtered through kieselguhr and the filtrate is concentrated completely by rotary evaporation i. V.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08772323B2 |
| Source dataset | uspto-grants-2014_07 |
| ORD ID | ord-6b136be23d0844fe8f7d4c78d963c661 |
| Source note | uspto-grants-2014_07 |