Lawesson's reagent → HCID 86689074, compound

Participants

Reaction Conditions

Reaction Steps

680.00 mg (1.70 mmol) 2-(tert-butyl-dimethyl-silanyloxy)-1-(2-phenyl-6,7-dihydro-4H-oxazolo[5,4-c]pyridin-5-yl)-butan-1-one and 1.40 g (3.46 mmol) Lawesson's reagent are placed in 35 mL toluene and stirred overnight at 90° C. The solvent of the reaction mixture is eliminated in vacuo and the residue is purified on silica gel. (Eluant: cyclohexane/EA).

Provenance & Evidence