HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrazinecarboxylic acid, ethyl ester → HCID 86689076, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrazinecarboxylic acid, ethyl ester | HCID 20064 | — |
| Reactant | HCID 86689075 | HCID 86689075 | — |
| Catalyst | Mercurous acetate | HCID 61181 | — |
| Solvent | Tetrahydrofuran | HCID 8028 | — |
| Product | HCID 86689076 | HCID 86689076 | — |
Reaction Steps
185.00 mg (612 μmol) 2-hydroxy-1-(2-phenyl-6,7-dihydro-4H-oxazolo[5,4-c]pyridin-5-yl)-butan-1-thione, 70.00 mg (672 μmol) ethylhydrazinecarboxylate and 200.00 mg (628 μmol) mercury acetate are placed in 10 mL THF and the mixture is stirred for 2 h at RT. The reaction mixture is filtered through silica gel suction and the solvent is eliminated in vacuo.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08772323B2 |
| Source dataset | uspto-grants-2014_07 |
| ORD ID | ord-740acdbd5fe54a98adea71d2fa0aa4e9 |
| Source note | uspto-grants-2014_07 |