HuagongsheHuagongshe Chemistry Print Report · For research reference only
Cyclopropanesulfonyl chloride → HCID 56603048, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Cyclopropanesulfonyl chloride | HCID 2760919 | — |
| Reactant | HCID 66666483 | HCID 66666483 | — |
| Product | HCID 56603048 | HCID 56603048 | 17% |
Reaction Steps
Prepared according to Example 5 with 3-(2-methoxypyridin-3-yl)-4-phenoxybenzamide (Preparation 19, 0.030 g, 0.09 mmol) and cyclopropylsulfonyl chloride (0.030 g, 0.21 mmol). The product was purified by preparative HPLC to afford the title compound as a white solid (6.5 mg).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08772343B2 |
| Source dataset | uspto-grants-2014_07 |
| ORD ID | ord-a944cf37e8304f0c9a8047b954967528 |
| Source note | uspto-grants-2014_07 |