HuagongsheHuagongshe Chemistry Print Report · For research reference only
Propargylamine → HCID 178456890, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Propargylamine | HCID 239041 | — |
| Reactant | 4-Sulfanylidene-1,3-thiazolidin-2-one | HCID 1539595 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 178456890 | HCID 178456890 | — |
Reaction Steps
To a suspension of 4-thioxo-1,3-thiazolidin-2-one (12.8 g) in ethanol (200 mL) was added propargylamine (9.67 mL), and the mixture was stirred at room temperature overnight. The precipitate was collected by filtration, and washed with ethanol to give the title compound (11.9 g).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08772277B2 |
| Source dataset | uspto-grants-2014_07 |
| ORD ID | ord-68a8c3d249cf4a34bd24cbf400be7778 |
| Source note | uspto-grants-2014_07 |