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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1620490Generated: November 2, 2026

Ethoxyethylamine → HCID 178467931, compound

https://huagongshe.com/reaction/1620490

Reaction equation

Participants

RoleNameHCIDCharge
ReactantEthoxyethylamineHCID 66970—
Reactant4-Sulfanylidene-1,3-thiazolidin-2-oneHCID 1539595—
SolventEthanolHCID 702—
ProductHCID 178467931HCID 17846793185.6%

Reaction Steps

To a solution of 2-ethoxyethanamine (4.07 g) in ethanol (100 mL) was added 4-thioxo-1,3-thiazolidin-2-one (4.05 g), and the mixture was stirred at room temperature overnight. The reaction mixture was concentrated, and the residue was purified by silica gel column chromatography (ethyl acetate/hexane) to give the title compound (4.90 g).

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS08772277B2
Source datasetuspto-grants-2014_07
ORD IDord-cc5f7d83498a4c6a9e0b61fcef548c39
Source noteuspto-grants-2014_07