HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ethoxyethylamine → HCID 178467931, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ethoxyethylamine | HCID 66970 | — |
| Reactant | 4-Sulfanylidene-1,3-thiazolidin-2-one | HCID 1539595 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 178467931 | HCID 178467931 | 85.6% |
Reaction Steps
To a solution of 2-ethoxyethanamine (4.07 g) in ethanol (100 mL) was added 4-thioxo-1,3-thiazolidin-2-one (4.05 g), and the mixture was stirred at room temperature overnight. The reaction mixture was concentrated, and the residue was purified by silica gel column chromatography (ethyl acetate/hexane) to give the title compound (4.90 g).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08772277B2 |
| Source dataset | uspto-grants-2014_07 |
| ORD ID | ord-cc5f7d83498a4c6a9e0b61fcef548c39 |
| Source note | uspto-grants-2014_07 |