HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-Sulfanylidene-1,3-thiazolidin-2-one → HCID 178518038, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-Sulfanylidene-1,3-thiazolidin-2-one | HCID 1539595 | — |
| Reactant | 3-Oxetanamine | HCID 9833923 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 178518038 | HCID 178518038 | 82.4% |
Reaction Steps
To a solution of oxetane-3-amine (4.94 g) in ethanol (60 mL) was added 4-thioxo-1,3-thiazolidin-2-one (6 g), and the mixture was stirred at room temperature for 30 min. The precipitate was collected by filtration and washed with ethanol to give the title compound (6.39 g).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08772277B2 |
| Source dataset | uspto-grants-2014_07 |
| ORD ID | ord-3aac99eb3b1942bd86d553563b6cd1e1 |
| Source note | uspto-grants-2014_07 |