HuagongsheHuagongshe Chemistry Print Report · For research reference only
Cyclopropanemethanamine → HCID 178518077, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Cyclopropanemethanamine | HCID 75646 | — |
| Reactant | 4-Sulfanylidene-1,3-thiazolidin-2-one | HCID 1539595 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 178518077 | HCID 178518077 | 42.9% |
Reaction Steps
To a solution of 1-cyclopropylmethanamine (2.34 g) in ethanol (100 mL) was added 4-thioxo-1,3-thiazolidin-2-one (2.92 g), and the mixture was stirred at room temperature overnight. The solvent was evaporated under reduced pressure and washed with ethanol to give the title compound (1.60 g).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08772277B2 |
| Source dataset | uspto-grants-2014_07 |
| ORD ID | ord-0c679eef303344adb920d1ad4191852b |
| Source note | uspto-grants-2014_07 |