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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1620522Generated: October 28, 2026

2-(2-Methoxyethoxy)ethanamine → HCID 178496228, compound

https://huagongshe.com/reaction/1620522

Reaction equation

Participants

RoleNameHCIDCharge
Reactant2-(2-Methoxyethoxy)ethanamineHCID 520530—
Reactant4-Sulfanylidene-1,3-thiazolidin-2-oneHCID 1539595—
SolventEthanolHCID 702—
ProductHCID 178496228HCID 17849622884.4%

Reaction Steps

To a solution of 4-thioxo-1,3-thiazolidin-2-one (2.24 g) in ethanol (20 mL) was added 2-(2-methoxyethoxy)ethanamine (2.5 g), and the mixture was stirred at room temperature for 5 hr. The solvent was evaporated under reduced pressure, and the residue was purified by silica gel column chromatography (ethyl acetate) to give the title compound (3.1 g).

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS08772277B2
Source datasetuspto-grants-2014_07
ORD IDord-5cf11b4d936848579ae1dbc183df1ea3
Source noteuspto-grants-2014_07