HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-Sulfanylidene-1,3-thiazolidin-2-one → HCID 178518029, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-Sulfanylidene-1,3-thiazolidin-2-one | HCID 1539595 | — |
| Reactant | Oxolan-3-amine | HCID 3365553 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 178518029 | HCID 178518029 | 57.5% |
Reaction Steps
To a solution of tetrahydrofuran-3-amine (2.94 g) in ethanol (20 mL) was added 4-thioxo-1,3-thiazolidin-2-one (3.0 g), and the mixture was stirred at room temperature for 1 hr. The precipitate was collected by filtration and washed with ethanol to give the title compound (2.41 g).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08772277B2 |
| Source dataset | uspto-grants-2014_07 |
| ORD ID | ord-0edba349bd934a568ea919642327b378 |
| Source note | uspto-grants-2014_07 |