HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 86678720, compound → [2-(2-aminoethoxy)ethyl]diethylamine
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 86678720 | HCID 86678720 | — |
| Solvent | Hydrogen chloride-ethyl acetate | HCID 21866389 | — |
| Product | [2-(2-aminoethoxy)ethyl]diethylamine | HCID 15105206 | 96.1% |
Reaction Steps
A mixed solution of tert-butyl {2-[2-(diethylamino)ethoxy]ethyl}carbamate (3.77 g) and 4M hydrogen chloride/ethyl acetate solution (40 mL) was stirred at room temperature for 3 hr, and the solvent was evaporated under reduced pressure. The residue was purified by silica gel column chromatography (NH, methanol/ethyl acetate) to give the title compound (2.23 g).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08772277B2 |
| Source dataset | uspto-grants-2014_07 |
| ORD ID | ord-677aa69319024a308fd387f0c5064131 |
| Source note | uspto-grants-2014_07 |