HuagongsheHuagongshe Chemistry Print Report · For research reference only
Triethylamine → HCID 178514027, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Triethylamine | HCID 8471 | — |
| Reactant | 4-Sulfanylidene-1,3-thiazolidin-2-one | HCID 1539595 | — |
| Reactant | Glycinamide hydrochloride | HCID 2723639 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 178514027 | HCID 178514027 | 99.6% |
Reaction Steps
To a solution of glycinamide hydrochloride (5.00 g) and triethylamine (6.30 mL) in ethanol (60 mL) was added 4-thioxo-1,3-thiazolidin-2-one (5.02 g), and the mixture was stirred at room temperature overnight. The precipitate was collected by filtration and washed with ethanol to give the title compound (6.50 g).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08772277B2 |
| Source dataset | uspto-grants-2014_07 |
| ORD ID | ord-ff40eac016ab43f0ae9252c622e3063a |
| Source note | uspto-grants-2014_07 |