HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-amino-N-methylacetamide → HCID 178485783, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-amino-N-methylacetamide | HCID 89675 | — |
| Reactant | 4-Sulfanylidene-1,3-thiazolidin-2-one | HCID 1539595 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 178485783 | HCID 178485783 | 87.2% |
Reaction Steps
To a solution of N-methylglycinamide (4.06 g) in ethanol (22 mL) was added 4-thioxo-1,3-thiazolidin-2-one (5.11 g), and the mixture was stirred at room temperature for 4 hr. The precipitate was collected by filtration and washed with ethanol to give the title compound (6.26 g).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08772277B2 |
| Source dataset | uspto-grants-2014_07 |
| ORD ID | ord-6fecd994a4174d7dbf1e052df28e6e3c |
| Source note | uspto-grants-2014_07 |