HuagongsheHuagongshe Chemistry Print Report · For research reference only
Propargylamine → HCID 178456888, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Propargylamine | HCID 239041 | — |
| Reactant | 4-Sulfanylidene-1,3-oxazolidin-2-one | HCID 15292581 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 178456888 | HCID 178456888 | 79.1% |
Reaction Steps
To a solution of 4-thioxooxazolidin-2-one (180 mg) in ethanol (3 mL) was added prop-2-yn-1-amine (85 mg) at room temperature. The reaction mixture was stirred at room temperature for 2 hr. The precipitated white solid was collected by filtration, and washed with ethyl acetate/hexane to give the title compound (168 mg).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08772277B2 |
| Source dataset | uspto-grants-2014_07 |
| ORD ID | ord-095f6179a7b64a089501c0b012bfefa7 |
| Source note | uspto-grants-2014_07 |