HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 86678817, compound → HCID 86678816, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 86678817 | HCID 86678817 | — |
| Catalyst | HCID 178418390 | HCID 178418390 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 86678816 | HCID 86678816 | 104.3% |
Reaction Steps
A solution of (R)-benzyl[1-(dimethylamino)-3-hydroxy-1-oxopropan-2-yl]carbamate (1.30 g) and 10% palladium carbon (130 mg) in methanol (30 mL) was stirred at room temperature for 7 hr under a hydrogen atmosphere. The reaction mixture was filtered, and the filtrate was concentrated under reduced pressure to give the title compound (673 mg).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08772277B2 |
| Source dataset | uspto-grants-2014_07 |
| ORD ID | ord-d40d4c0d133e4d8699d273a2f6d7183e |
| Source note | uspto-grants-2014_07 |