Cyclohexylamine → HCID 178517975, compound

Participants

Reaction Steps

To a solution of 4-thioxo-1,3-thiazolidin-2-one (1.00 g) in ethanol (30 mL) was added cyclohexylamine (0.88 mL), and the mixture was heated under reflux overnight. The reaction mixture was concentrated under reduced pressure, the residue was purified by silica gel column chromatography (ethyl acetate/hexane), and the obtained powder was washed with ethyl acetate to give the title compound (599 mg).

Provenance & Evidence