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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1620680Generated: November 1, 2026

HCID 86678841, compound → HCID 45087500, compound

https://huagongshe.com/reaction/1620680

Reaction equation

Participants

RoleNameHCIDCharge
ReactantHCID 86678841HCID 86678841—
CatalystHCID 178418390HCID 178418390—
SolventMethanolHCID 887—
ProductHCID 45087500HCID 45087500101.4%

Reaction Steps

A solution of (S)-benzyl[1-(dimethylamino)-3-hydroxy-1-oxopropan-2-yl]carbamate (3.20 g) and 10% palladium carbon (320 mg) in methanol (30 mL) was stirred at room temperature for 5 hr under a hydrogen atmosphere. The reaction mixture was filtered, and the filtrate was concentrated under reduced pressure to give the title compound (1.61 g).

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS08772277B2
Source datasetuspto-grants-2014_07
ORD IDord-e7a15c9f9d9f46c3bafa3c3e8aa2fd5a
Source noteuspto-grants-2014_07