HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 86678841, compound → HCID 45087500, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 86678841 | HCID 86678841 | — |
| Catalyst | HCID 178418390 | HCID 178418390 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 45087500 | HCID 45087500 | 101.4% |
Reaction Steps
A solution of (S)-benzyl[1-(dimethylamino)-3-hydroxy-1-oxopropan-2-yl]carbamate (3.20 g) and 10% palladium carbon (320 mg) in methanol (30 mL) was stirred at room temperature for 5 hr under a hydrogen atmosphere. The reaction mixture was filtered, and the filtrate was concentrated under reduced pressure to give the title compound (1.61 g).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08772277B2 |
| Source dataset | uspto-grants-2014_07 |
| ORD ID | ord-e7a15c9f9d9f46c3bafa3c3e8aa2fd5a |
| Source note | uspto-grants-2014_07 |