HCID 71247139, compound → HCID 71352300, compound

Participants

Reaction Steps

To a solution of benzyl[(2S)-1,4-bis(dimethylamino)-1,4-dioxobutan-2-yl]carbamate (550 mg) in ethanol (5 mL) was added 10% palladium carbon (182 mg) at room temperature. The reaction mixture was stirred at room temperature for 5 hr under a hydrogen atmosphere. The solid was removed by filtration, and the filtrate was concentrated under reduced pressure to give the title compound (350 mg).

Provenance & Evidence