HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-Sulfanylidene-1,3-thiazolidin-2-one → HCID 178504888, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-Sulfanylidene-1,3-thiazolidin-2-one | HCID 1539595 | — |
| Reactant | 2-(Methylsulfonyl)ethanamine | HCID 4340561 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 178504888 | HCID 178504888 | 96.3% |
Reaction Steps
To a solution of 4-thioxo-1,3-thiazolidin-2-one (865 mg) in ethanol (10 mL) was added 2-(methylsulfonyl)ethanamine (1 g), and the mixture was stirred at room temperature for 3 hr. The precipitate was collected by filtration to give the title compound (1.39 g).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08772277B2 |
| Source dataset | uspto-grants-2014_07 |
| ORD ID | ord-368306d308d64498ac0fca6e607fbb3e |
| Source note | uspto-grants-2014_07 |