HuagongsheHuagongshe Chemistry Print Report · For research reference only
3-Amino-1-propanol → HCID 178518141, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 3-Amino-1-propanol | HCID 9086 | — |
| Reactant | 4-Sulfanylidene-1,3-thiazolidin-2-one | HCID 1539595 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 178518141 | HCID 178518141 | 77.6% |
Reaction Steps
To a solution of 4-thioxothiazolidin-2-one (2.66 g) in ethanol (50 mL) was added 3-aminopropan-1-ol (1.50 g) at room temperature. The reaction mixture was stirred at room temperature for 4 hr, the solvent was evaporated under reduced pressure, and the residue was purified by silica gel column chromatography (NH, methanol/ethyl acetate) to give the title compound (2.70 g).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08772277B2 |
| Source dataset | uspto-grants-2014_07 |
| ORD ID | ord-06d7b931519a4ee580935bb6927e82c5 |
| Source note | uspto-grants-2014_07 |