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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1620766Generated: November 1, 2026

HCID 86678926, compound → HCID 86678927, compound

https://huagongshe.com/reaction/1620766

Reaction equation

Participants

RoleNameHCIDCharge
ReactantHCID 86678926HCID 86678926—
CatalystHCID 178418390HCID 178418390—
SolventEthanolHCID 702—
ProductHCID 86678927HCID 8667892758.4%

Reaction Steps

To a solution of benzyl[(1S)-2-(dimethylamino)-1-(1-hydroxycyclopropyl)-2-oxoethyl]carbamate (190 mg) in ethanol (5 mL) was added 10% palladium carbon (69 mg) at room temperature. The reaction mixture was stirred at room temperature for 5 hr under a hydrogen atmosphere. The reaction mixture was filtered, and the filtrate was concentrated under reduced pressure to give the title compound (60 mg).

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS08772277B2
Source datasetuspto-grants-2014_07
ORD IDord-a6aec1674a4342679378c216bd8f6d11
Source noteuspto-grants-2014_07