HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 25529914, compound → HCID 14963842, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 25529914 | HCID 25529914 | — |
| Catalyst | HCID 178418390 | HCID 178418390 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 14963842 | HCID 14963842 | 79.9% |
Reaction Steps
A solution of benzyl[(2S)-3-methyl-1-(morpholin-4-yl)-1-oxobutan-2-yl]carbamate (1.83 g) and 10% palladium carbon (0.608 g) in ethanol (30 mL) was stirred at room temperature overnight under a hydrogen atmosphere. The reaction mixture was filtered, and the filtrate was concentrated under reduced pressure to give the title compound (850 mg).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08772277B2 |
| Source dataset | uspto-grants-2014_07 |
| ORD ID | ord-3848dc638f7d40dc9d6880bb55e96593 |
| Source note | uspto-grants-2014_07 |