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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1620770Generated: November 1, 2026

HCID 25529914, compound → HCID 14963842, compound

https://huagongshe.com/reaction/1620770

Reaction equation

Participants

RoleNameHCIDCharge
ReactantHCID 25529914HCID 25529914—
CatalystHCID 178418390HCID 178418390—
SolventEthanolHCID 702—
ProductHCID 14963842HCID 1496384279.9%

Reaction Steps

A solution of benzyl[(2S)-3-methyl-1-(morpholin-4-yl)-1-oxobutan-2-yl]carbamate (1.83 g) and 10% palladium carbon (0.608 g) in ethanol (30 mL) was stirred at room temperature overnight under a hydrogen atmosphere. The reaction mixture was filtered, and the filtrate was concentrated under reduced pressure to give the title compound (850 mg).

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS08772277B2
Source datasetuspto-grants-2014_07
ORD IDord-3848dc638f7d40dc9d6880bb55e96593
Source noteuspto-grants-2014_07