HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-Sulfanylidene-1,3-thiazolidin-2-one → HCID 178463636, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-Sulfanylidene-1,3-thiazolidin-2-one | HCID 1539595 | — |
| Reactant | Ethanamine ethanol | HCID 22128961 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 178463636 | HCID 178463636 | 46.2% |
Reaction Steps
To a solution of 4-thioxo-1,3-thiazolidin-2-one (640 mg) in ethanol (6 mL) was added 30% ethanamine ethanol solution (722 mg), and the mixture was stirred at room temperature for 3 hr. The reaction mixture was concentrated under reduced pressure, and the residue was washed with 2-propanol to give the title compound (320 mg).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08772277B2 |
| Source dataset | uspto-grants-2014_07 |
| ORD ID | ord-47ca4d38006f46fdb020a1f1380f1e4c |
| Source note | uspto-grants-2014_07 |