HuagongsheHuagongshe Chemistry Print Report · For research reference only
Propylamine → HCID 178456891, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Propylamine | HCID 7852 | — |
| Reactant | 4-Sulfanylidene-1,3-thiazolidin-2-one | HCID 1539595 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 178456891 | HCID 178456891 | — |
Reaction Steps
To a solution of 4-thioxo-1,3-thiazolidin-2-one (640 mg) in ethanol (6 mL) was added propan-1-amine (0.397 mL), and the mixture was stirred at room temperature for 3 hr. The reaction mixture was concentrated under reduced pressure, and the residue was purified by silica gel column chromatography (ethyl acetate/hexane) to give the title compound (450 mg).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08772277B2 |
| Source dataset | uspto-grants-2014_07 |
| ORD ID | ord-091b134e1b4248c5a8c1757b0a2ef3c0 |
| Source note | uspto-grants-2014_07 |