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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1620781Generated: November 2, 2026

Propylamine → HCID 178456891, compound

https://huagongshe.com/reaction/1620781

Reaction equation

Participants

RoleNameHCIDCharge
ReactantPropylamineHCID 7852—
Reactant4-Sulfanylidene-1,3-thiazolidin-2-oneHCID 1539595—
SolventEthanolHCID 702—
ProductHCID 178456891HCID 178456891—

Reaction Steps

To a solution of 4-thioxo-1,3-thiazolidin-2-one (640 mg) in ethanol (6 mL) was added propan-1-amine (0.397 mL), and the mixture was stirred at room temperature for 3 hr. The reaction mixture was concentrated under reduced pressure, and the residue was purified by silica gel column chromatography (ethyl acetate/hexane) to give the title compound (450 mg).

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS08772277B2
Source datasetuspto-grants-2014_07
ORD IDord-091b134e1b4248c5a8c1757b0a2ef3c0
Source noteuspto-grants-2014_07