HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-{[4-(Methylsulfinyl)-1,3-thiazol-2-yl]carbamoyl}phenyl acetate → 3-{[4-(Methylsulfinyl)-1,3-thiazol-2-yl]carbamoyl}phenyl acetate
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-{[4-(Methylsulfinyl)-1,3-thiazol-2-yl]carbamoyl}phenyl acetate | HCID 56969389 | — |
| Reactant | 3-{[4-(Methylthio)-1,3-thiazol-2-yl]carbamoyl}phenyl acetate | HCID 57571980 | — |
| Product | 3-{[4-(Methylsulfinyl)-1,3-thiazol-2-yl]carbamoyl}phenyl acetate | HCID 56969391 | — |
Reaction Steps
Using the above procedure for compound (3), 513 (0.61 g, 2.0 mmol) gives crude 5 as a white solid. The crude product is stirred in diethyl ether (30 mL) for 30 minutes, filtered and air dried to give 5 as a white solid.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08772502B2 |
| Source dataset | uspto-grants-2014_07 |
| ORD ID | ord-03823bb81c1d4962baaddc978b0568cf |
| Source note | uspto-grants-2014_07 |