Hydrochloric Acid → HCID 86677479, compound

Participants

Reaction Steps

5-[2-Bis(tert-butoxycarbonyl)aminoethyl]-1-methyl-3-pyridin-3-yl-[1,2,4]triazole (133 mg, 330 μmol) was suspended in hydrochloric acid (4M solution in dioxane, 2 mL, 8.00 mmol) and the mixture was stirred at r. t. for 1 h. The reaction mixture was evaporated and dried to give the product as colorless solid (118 mg, 342 μmol, 104%) which was used without any further purification for the next step. MS: M=204.2 (M+H)+

Provenance & Evidence