HuagongsheHuagongshe Chemistry Print Report · For research reference only
N-((1,1-dimethylethoxy)carbonyl)-beta-alanine → HCID 8734373, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | N-((1,1-dimethylethoxy)carbonyl)-beta-alanine | HCID 76809 | — |
| Reactant | Bromomethyl 2-methoxyphenyl ketone | HCID 123440 | — |
| Product | HCID 8734373 | HCID 8734373 | — |
Reaction Steps
The product was obtained starting from 3-(tert-butoxycarbonylamino)propanoic acid (400 mg, 2.11 mmol) and 2-bromo-1-(2-methoxyphenyl)ethanone (484 mg, 2.11 mmol) according to the method described in example 7, step 1 as black oil (786 mg, 2.1 mmol, 99.2%). MS: M=238.2 (M-Boc+H)+
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08772510B2 |
| Source dataset | uspto-grants-2014_07 |
| ORD ID | ord-9c3dbe2b449d43a2946e0d35dd444649 |
| Source note | uspto-grants-2014_07 |