HCID 21758136, compound → HCID 71279122, compound

Participants

Reaction Conditions

Reaction Steps

The product was obtained starting from 1,2-dimethyl-1H-imidazole-4,5-dicarboxylic acid 4-methyl ester (100 mg, 505 μmol; example 8, steps 1-2) and 2-(1-methyl-4-phenyl-1H-imidazol-2-yl)ethanamine dihydrochloride (152 mg, 555 μmol; example 7, steps 1-4) according to the method described in example 10, step 5 after stirring at 70° C. for 16 h, aqueous workup and purification as light yellow oil (111 mg, 291 μmol, 57.7%). MS: M=382.4 (M+H)+

Provenance & Evidence