HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 21758136, compound → HCID 71279172, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 21758136 | HCID 21758136 | — |
| Reactant | HCID 86677489 | HCID 86677489 | — |
| Product | HCID 71279172 | HCID 71279172 | — |
Reaction Steps
The product was obtained starting from lithium 4-(methoxycarbonyl)-1-methyl-1H-1,2,3-triazole-5-carboxylate (150 mg, 785 μmol) and 2-(1-methyl-4-phenyl-1H-imidazol-2-yl)ethanamine dihydrochloride (226 mg, 824 μmol, example 7, step 4) according to the method described in example 7, step 5 after aqueous work-up and purification by flash chromatography (using silica gel and an ethyl acetate/heptane gradient) as light yellow solid (79 mg, 214 μmol, 27.3%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08772510B2 |
| Source dataset | uspto-grants-2014_07 |
| ORD ID | ord-350a20c0bd644ea7ba1d97449df45ff2 |
| Source note | uspto-grants-2014_07 |