HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 21758136, compound → HCID 71279099, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 21758136 | HCID 21758136 | — |
| Reactant | HCID 71279098 | HCID 71279098 | — |
| Product | HCID 71279099 | HCID 71279099 | — |
Reaction Steps
The product was obtained starting from 4-(methoxycarbonyl)-1-methyl-2-(trifluoromethyl)-1H-imidazole-5-carboxylic acid (200 mg, 793 μmol) and 2-(1-methyl-4-phenyl-1H-imidazol-2-yl)ethanamine hydrochloride (226 mg, 952 μmol, example 7, step 4) according to the method described in example 7, step 5 after aqueous work-up and purification by flash chromatography (using silica gel and an ethyl acetate/heptane gradient) as white foam (128 mg, 294 μmol, 37.1%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08772510B2 |
| Source dataset | uspto-grants-2014_07 |
| ORD ID | ord-fa1e9d7d334c4d3cb68b1d19bc66bdc7 |
| Source note | uspto-grants-2014_07 |