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HRID1621192

反应详情

EQUATION

反应方程式

HRID 1621192 的结构方程式

REACTANTS

反应物

2
结构：CCCCCC(N)=O
HCID12332

Hexanamide

C6H13NO

结构：CCN(CC)c1ccc(C=O)cc1
HCID67114

4-(Diethylamino)benzaldehyde

C11H15NO

PRODUCTS

生成物

1
结构：CCCCCC(=O)NC(NC(=O)CCCCC)c1ccc(N(CC)CC)cc1
HCID71460951

未命名化合物

收率 76%

PROCEDURE

实验过程

Compound 53 was prepared from hexanamide and 4-(diethylamino)benzaldehyde using method 1. Yield: 76%. 1H NMR (400 MHz, CD3OD) δ 7.19 (d, J=8.8 Hz, 2H), 6.71 (d, J=8.8 Hz, 2H), 6.58 (t, J=8.4 Hz, 1H), 3.35-3.41 (m, 4H), 2.19-2.26 (m, 4H), 1.61-1.68 (m, 4H), 1.32-1.35 (m, 8H), 1.14 (t, J=6.8 Hz, 6H), 0.94 (t, J=2.8 Hz, 6H). LC-MS (ESI): m/z 390.3 (M+H)+. HRMS (ESI) for C23H40N3O2 (MH+): calcd, 390.3115. found 390.3108.