HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hexanamide → N,N'-((4-(diethylamino)phenyl)methylene)dihexanamide
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hexanamide | HCID 12332 | — |
| Reactant | 4-(Diethylamino)benzaldehyde | HCID 67114 | — |
| Product | N,N'-((4-(diethylamino)phenyl)methylene)dihexanamide | HCID 71460951 | 76% |
Reaction Steps
Compound 53 was prepared from hexanamide and 4-(diethylamino)benzaldehyde using method 1. Yield: 76%. 1H NMR (400 MHz, CD3OD) δ 7.19 (d, J=8.8 Hz, 2H), 6.71 (d, J=8.8 Hz, 2H), 6.58 (t, J=8.4 Hz, 1H), 3.35-3.41 (m, 4H), 2.19-2.26 (m, 4H), 1.61-1.68 (m, 4H), 1.32-1.35 (m, 8H), 1.14 (t, J=6.8 Hz, 6H), 0.94 (t, J=2.8 Hz, 6H). LC-MS (ESI): m/z 390.3 (M+H)+. HRMS (ESI) for C23H40N3O2 (MH+): calcd, 390.3115. found 390.3108.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08772541B2 |
| Source dataset | uspto-grants-2014_07 |
| ORD ID | ord-89e4624de9a14678b744ce17a45f567e |
| Source note | uspto-grants-2014_07 |