HCID 67022881, compound → HCID 25108974, compound

Participants

Reaction Steps

(2S,4R)-2-(4-Ethyl-phenylcarbamoyl)-4-(isoquinolin-6-ylamino)-pyrrolidine-1-carboxylic acid tert-butyl ester trifluoroacetate was dissolved in 4 N HCl in dioxane and stirred for 2 h at rt. Evaporation gave (2S,4R)-4-(Isoquinolin-6-ylamino)-pyrrolidine-2-carboxylic acid (4-ethyl-phenyl)-amide as the hydrochloride salt. Rt=1.05 min (Method A). Detected mass: 361.2 (M+H+).

Provenance & Evidence