HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrazine hydrate (1:1) → HCID 53403344, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrazine hydrate (1:1) | HCID 24654 | — |
| Reactant | Methyl N-methylindole-6-carboxylate | HCID 639843 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 53403344 | HCID 53403344 | — |
Reaction Steps
A mixture of 1-methyl-1H-indole-6-carboxylic acid methyl ester (3.2 g, 16.1 mmol), hydrazine monohydrate (8.5 g, 169 mmol) and methanol (50 ml) was stirred reflux for 15 h. The mixture was evaporated, water was added and the product was isolated by extraction with chloroform, followed by evaporation.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08778928B2 |
| Source dataset | uspto-grants-2014_07 |
| ORD ID | ord-ae8a9882e56440a585900b0b380268f3 |
| Source note | uspto-grants-2014_07 |