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HRID1622240

反应详情

EQUATION

反应方程式

HRID 1622240 的结构方程式

REACTANTS

反应物

2
结构：CS(=O)(=O)c1ccc(B(O)O)cc1
HCID2734364

4-(Methylsulfonyl)phenylboronic acid

C7H9BO4S

结构：CC(C)(C)OC(=O)N1CCC([C@]2(C)Cc3cc(Cl)ncc3O2)CC1
HCID86674904

未命名化合物

PRODUCTS

生成物

1
结构：CC(C)(C)OC(=O)N1CCC([C@]2(C)Cc3cc(-c4ccc(S(C)(=O)=O)cc4)ncc3O2)CC1
HCID57384100

未命名化合物

PROCEDURE

实验过程

The title compound is prepared from (S)-4-(5-chloro-2-methyl-2,3-dihydro-furo[2,3-c]pyridin-2-yl)-piperidine-1-carboxylic acid tert-butyl ester (Intermediate 29; the configuration of the stereocenter is arbitrarily assigned) and 4-(methanesulfonyl)phenylboronic acid following a procedure analogous to that described for Intermediate 7. LC (method 4): tR=1.19 min; Mass spectrum (ESI+): m/z=473 [m+H]+.