HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methanol → HCID 86656266, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methanol | HCID 887 | — |
| Reactant | Chloroform | HCID 6212 | — |
| Reactant | 1-Piperazinecarboxylic acid, 4-benzoyl-, 1,1-diMethylethyl ester | HCID 18519756 | — |
| Solvent | 1,4-Dioxane | HCID 31275 | — |
| Product | Hydrochloric Acid | HCID 313 | — |
| Product | HCID 86656266 | HCID 86656266 | 96% |
Reaction Steps
General procedure B was followed using tert-butyl 4-benzoylpiperazine-1-carboxylate 9 (75 mg, 0.26 mmol), MeOH (2 mL) and a 4 M solution of hydrogen chloride in 1,4-dioxane (2 mL) to furnish the title compound as a colourless oil (47 mg, 96%), umax (CHCl3)/cm−1 3015, 2954, 1622, 1435, 1290, 1136, 1018; m/z (ESI) C11H15N2O requires 191.1179, found [M+H]+ 191.1179.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08778925B2 |
| Source dataset | uspto-grants-2014_07 |
| ORD ID | ord-3c9adf21c5944c05a736a844dcad0743 |
| Source note | uspto-grants-2014_07 |